Preparation and characterization of inclusion complexes of β-cyclodextrin with 1-butyl-3-methylimidazolium tetrafluoroborate ([bmim][bf4])ionic liquid / Norashikin bt Othman

The interaction between β-cyclodextrin and ionic liquid 1-butyl-3-methylimidazolium tetrafluoroborate ([Bmim][BF4]) had been studied. The inclusion complexation interaction was confirmed by FT-IR spectra. The inclusion complex was also characterized by 1H NMR, TGA and DSC. The results showed that...

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தலைமை எழுத்தாளர்: Othman, Norashikin
வடிவம்: Thesis
வெளியீடப்பட்டது: 2013
பகுதிகள்:
நிகழ்நிலை அணுகல்:http://studentsrepo.um.edu.my/4527/
http://studentsrepo.um.edu.my/4527/2/CONTENTS_%26_ABSTRACT_(Norashikin_Othman).pdf
http://studentsrepo.um.edu.my/4527/1/CD%2DIL_INCLUSION_COMPLEXES_(Norashikin_Othman).pdf
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தொகுப்பு:The interaction between β-cyclodextrin and ionic liquid 1-butyl-3-methylimidazolium tetrafluoroborate ([Bmim][BF4]) had been studied. The inclusion complexation interaction was confirmed by FT-IR spectra. The inclusion complex was also characterized by 1H NMR, TGA and DSC. The results showed that the host-guest system presented a channel type structure and each glucose unit of β-cyclodextrin was in similar environment. The decomposition temperature of inclusion complex was lower than that of [bmim][BF4] and β- cyclodextrin individually. The ratio of 1:1 inclusion complex was determined in this study.