The effect of halloysite and boron nitride as nucleating agents on the crystallization of poly (3- hydroxybutyrate)

The crystallization behaviour of Poly(3-hydroxybutyrate) (PHB) induced by two kinds of nucleating agents which are Boron Nitride (BN) and Halloysite nanotubes (HNT) was investigated using Differential Scanning Calorimetry (DSC). PHB composites with 2, 4, 6, 8 wt% of BN and HNT were prepared by melt...

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Bibliographic Details
Main Authors: Mat Yusof, Nur Nadia, Othman, Norhayani, Samsudin, Sani Amril
Format: Conference or Workshop Item
Published: 2015
Subjects:
Online Access:http://eprints.utm.my/63458/
http://eprints.utm.my/63458/
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Summary:The crystallization behaviour of Poly(3-hydroxybutyrate) (PHB) induced by two kinds of nucleating agents which are Boron Nitride (BN) and Halloysite nanotubes (HNT) was investigated using Differential Scanning Calorimetry (DSC). PHB composites with 2, 4, 6, 8 wt% of BN and HNT were prepared by melt mixing. Presence of 8wt% BN in PHB significantly enhanced the melting temperature (Tm) and also accelerates the crystallization temperature (Tc) of PHB. Meanwhile, addition of more than 2wt% of HNT reduced the Tc thus crystallization of PHB/HNT composites. Even, the crystallization of composites with 8wt% HNT is slower than 8wt% BN but still faster than pure PHB. The degree of crystallinity (Xc) also was calculated from the DSC results.